Reading materials on NMR and Crystallography methods.

Crystallography

Crystallization and Condition Screening

Calero G, Cohen AE, Luft JR, Newman J, and Snell EH. "Identifying, studying and making good use of macromolecular crystals". Acta Cryst. F 2014 (F70): p 993-1008. DOI: 10.1107/S2053230X14016574

Collecting Diffraction Data

Mueller M, Wang M, and Schulze-Briese C. "Optimal fine φ-slicing for single-photon-counting pixel detectors". Acta Cryst. D 2012 (D68): p 42-56. DOI: 10.1107/S0907444911049833

Krojer T, Pike ACW, and von Delft F. "Squeezing the most from every crystal: the fine details of data collection." Acta Cryst. D 2013 (D69): p 1303-13. DOI: 10.1107/S0907444913013280

NMR

Chemical Exchange

Wang C, Rance M, Palmer AG III. "Mapping chemical exchange in proteins with MW > 50 kD." J Am. Chem. Soc. 2003 (125): p 8968-9. DOI: 10.1021/ja035139z

Kneller JM, Lu M, and Bracken C. "An effective method for the discrimination of motional anisotropy and chemical exchange". J. Am. Chem. Soc. 2002 (124): p 1852-3. DOI: 10.1021/ja017461k

Dynamics Models

Lipari G and Szabo A. "Model-free approach to the interpretation of nuclear magnetic resonance relaxation in macromolecules. 1. Theory and range of validity".  J. Am. Chem. Soc. 1982 (104): p 4546-4559. DOI: 10.1021/ja00381a009