Reading materials on NMR and Crystallography methods.
Crystallography
Crystallization and Condition Screening
Calero G, Cohen AE, Luft JR, Newman J, and Snell EH. "Identifying, studying and making good use of macromolecular crystals". Acta Cryst. F 2014 (F70): p 993-1008. DOI: 10.1107/S2053230X14016574
Collecting Diffraction Data
Mueller M, Wang M, and Schulze-Briese C. "Optimal fine φ-slicing for single-photon-counting pixel detectors". Acta Cryst. D 2012 (D68): p 42-56. DOI: 10.1107/S0907444911049833
Krojer T, Pike ACW, and von Delft F. "Squeezing the most from every crystal: the fine details of data collection." Acta Cryst. D 2013 (D69): p 1303-13. DOI: 10.1107/S0907444913013280
NMR
Chemical Exchange
Wang C, Rance M, Palmer AG III. "Mapping chemical exchange in proteins with MW > 50 kD." J Am. Chem. Soc. 2003 (125): p 8968-9. DOI: 10.1021/ja035139z
Kneller JM, Lu M, and Bracken C. "An effective method for the discrimination of motional anisotropy and chemical exchange". J. Am. Chem. Soc. 2002 (124): p 1852-3. DOI: 10.1021/ja017461k
Dynamics Models
Lipari G and Szabo A. "Model-free approach to the interpretation of nuclear magnetic resonance relaxation in macromolecules. 1. Theory and range of validity". J. Am. Chem. Soc. 1982 (104): p 4546-4559. DOI: 10.1021/ja00381a009