The The Chemistry Department currently has four Bruker high field NMR spectrometers: one 600Megahertz (MHz), one 300 MHz and two 400 MHz instruments. In addition there are two Bruker data processing stations. The 600, both 400s, and the processing stations are located in GeoChem 410 and the remaining 300 is located in MacMillan 315.
The website for making reservations on the NMR spectrometers is http://faces.ccrc.uga.edu.
To use the instruments, one must attend a training class and be issued a computer login with password. If you are interested in attending a training session, please contact facilities supervisor Russ Hopson.
Names and Locations of the NMRs in the Brown NMR Facility:
NAME
|
LOCATION
|
PROBE
|
BEST NMR FOR
|
|
ZEUS |
GC410 - 400MHz Furthest from Door on Left |
z-BBO |
13C, (all nuclei except 1H) |
|
ARTEMIS |
GC410 - 400MHz Closest to Door on Left |
z-BBFO |
13C, (all nuclei except 1H) |
|
CRONUS |
GC410 - 600MHz Closest to Door on Right |
z-BBFO |
All Nuclei |
|
ARIES |
MM315 |
z-BBI |
1H, HSQC,HMBC |
|
HELIOS |
GC410 - Processing Station Closest to Door |
|
|
|
Caerus |
GC410 - Processing Station Furthest from Door |
|
NOTE: A 10ul Capillary NMR Probe an a 5mm z-TXI are available for the 400MHz spectrometers and can be installed upon request. A 600 MHz z-BBO that can lock on 19F on the 1H channel, and observe 2H on the BB channel, as well as a z-TXI probe are available for the 600 MHz Spectrometer.
- How to setup and aquire a 1-D 1H and 13C NMR with Topspin
- How to measure T1
- How to measure T2
- How to setup and aquire COSY experiments with Topspin on ZEUS, ARTEMIS, and HADES
- How to setup and aquire COSY experiments with Topspin on ARIES
- How to setup and acquire HMQC or HSQC experiments on ZEUS, ARTEMIS, and HADES
- How to setup and acquire HMBC experiments on ZEUS, ARTEMIS, and HADES
- How to setup and acquire NOESY experiments on ZEUS, ARTEMIS, and HADES
- How to setup and acquire 1-D NOE Difference/Gradient NOE experiments on ZEUS/ARTEMIS/HADES
- How to setup and acquire a 1-D TOCSY on ZEUS and ARTEMIS
- How to setup and acquire Diffusion Experiments on ZEUS, ARTEMIS, and HADES
- How to setup and acquire using Solvent Suppression
- How to Observe 19F on ARIES
- How to Observe 2H NMR
- How to use the CapNMR Probe
- How to run the ICONNMR
- How to perform variable temperature experiments
- Brown NMR Facility Magnet Specs
- Bruker Manual
- Magnet Safety Documentation
- Saving NMR data to USB Drives
- Saving NMR by SSH
- Transferring Files
- NMR processing software is available from MESTREC.
- Introductory NMR Lecture
Contact Information:
Russell Hopson, Ph.D.
Mass Spectrometer Specialist